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pastafarian
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25 Oct 2011, 5:39 pm

I made some superconductors once, about 10 years old they worked really well and floated beautifully. got the recipe for Ytrium Barium Copper. All I remember is mixing it up, pressing it and cooking it in a furnace for days. it was quite straightfoward once you have found a suitable furnace. Liquid nitrogen is harder to come by.

Theres lots of recipes online that take you through it.

If you've got a local physics dept in a university nearby, or a science centre or museum, you might find someone with access to some liquid nitrogen that might help test. Maybe.



Fnord
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25 Oct 2011, 5:44 pm

Apple_in_my_Eye wrote:
"Any sufficiently advanced technology is indistinguishable from magic." -A.C.C.

The artist of Freefall put it all in one nice 'toon.

"Freefall" - (c) 1999
Image



Last edited by Fnord on 25 Oct 2011, 10:01 pm, edited 2 times in total.

Oodain
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25 Oct 2011, 6:00 pm

pastafarian wrote:
I made some superconductors once, about 10 years old they worked really well and floated beautifully. got the recipe for Ytrium Barium Copper. All I remember is mixing it up, pressing it and cooking it in a furnace for days. it was quite straightfoward once you have found a suitable furnace. Liquid nitrogen is harder to come by.

Theres lots of recipes online that take you through it.

If you've got a local physics dept in a university nearby, or a science centre or museum, you might find someone with access to some liquid nitrogen that might help test. Maybe.

i know a molecular biologist undergrad in odense university, i should ask her.

as i understand it you would actually need a substrate for the ytrrium alloy,

anyway i imagine the whole setup would take quite some time to get started, i would need to desinn a mold that can befilled and then pressed, in itself not easy.
though i dont know if it could be done with a hydraulic jack, we have some quite powerfull ones for lifting where i work, they can jack up at least 50t, making a press out of them would require a heavy framework though.


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HalibutSandwich
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25 Oct 2011, 8:36 pm

Oodain wrote:
as i understand it you would actually need a substrate for the ytrrium alloy,

anyway i imagine the whole setup would take quite some time to get started, i would need to desinn a mold that can befilled and then pressed, in itself not easy.
Can you make a 1 micron thick coating that way, or are you talking about making normal run-of-the-mill superconductors?

For high quality thin films it seems a popular way is a chemical deposition process using organometallic precursors. Apparently these methods don't require a vacuum and conversion temperature is only around 700 degC. I think you need an oxygen controlled atmosphere for the heat treating though. Coincidentally I met a guy recently that runs a metal factory and specializes in copper alloys. So they have controlled atmosphere furnaces for special annealing processes. Hmmm, maybe it's possible to do this.